Comparative hydrolysis analysis of cellulose samples and aspects of its application in conservation science

Manuel Becker; Kyujin Ahn; Markus Bacher; Chunlin Xu; Anna Sundberg; Stefan Willför; Thomas Rosenau; Antje Potthast

doi:10.1007/s10570-021-04048-6

Comparative hydrolysis analysis of cellulose samples and aspects of its application in conservation science

Manuel Becker, Kyujin Ahn, Markus Bacher, Chunlin Xu, Anna Sundberg, Stefan Willför, Thomas Rosenau, Antje Potthast^*

^*Tämän työn vastaava kirjoittaja

Tutkimustuotos: Lehtiartikkeli › Artikkeli › Tieteellinen › vertaisarvioitu

24 Sitaatiot (Scopus)

Abstrakti

Knowledge about the carbohydrate composition of pulp and paper samples is essential for their characterization, further processing, and understanding the properties. In this study, we compare sulfuric acid hydrolysis and acidic methanolysis, followed by GC–MS analysis of the corresponding products, by means of 42 cellulose and polysaccharide samples. Results are discussed and compared to solid-state NMR (crystallinity) and gel permeation chromatography (weight-averaged molecular mass) data. The use of the hydrolysis methods in the context of cellulose conservation science is evaluated, using e-beam treated and artificially aged cellulose samples.

Alkuperäiskieli	Englanti
Sivut	8719-8734
Sivumäärä	16
Julkaisu	Cellulose
Vuosikerta	28
Numero	13
Varhainen verkossa julkaisun päivämäärä	23 heinäk. 2021
DOI - pysyväislinkit	https://doi.org/10.1007/s10570-021-04048-6
Tila	Julkaistu - syysk. 2021
OKM-julkaisutyyppi	A1 Julkaistu artikkeli, soviteltu

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10.1007/s10570-021-04048-6

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abstract = "Knowledge about the carbohydrate composition of pulp and paper samples is essential for their characterization, further processing, and understanding the properties. In this study, we compare sulfuric acid hydrolysis and acidic methanolysis, followed by GC–MS analysis of the corresponding products, by means of 42 cellulose and polysaccharide samples. Results are discussed and compared to solid-state NMR (crystallinity) and gel permeation chromatography (weight-averaged molecular mass) data. The use of the hydrolysis methods in the context of cellulose conservation science is evaluated, using e-beam treated and artificially aged cellulose samples.",

keywords = "Cellulose, Crystallinity, Electron beam irradiation, Hemicellulose, Methanolysis, Sulfuric acid hydrolysis, Historic paper",

author = "Manuel Becker and Kyujin Ahn and Markus Bacher and Chunlin Xu and Anna Sundberg and Stefan Willf{\"o}r and Thomas Rosenau and Antje Potthast",

note = "Publisher Copyright: {\textcopyright} 2021, The Author(s).",

year = "2021",

month = sep,

doi = "10.1007/s10570-021-04048-6",

language = "English",

volume = "28",

pages = "8719--8734",

journal = "Cellulose",

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TY - JOUR

T1 - Comparative hydrolysis analysis of cellulose samples and aspects of its application in conservation science

AU - Becker, Manuel

AU - Ahn, Kyujin

AU - Bacher, Markus

AU - Xu, Chunlin

AU - Sundberg, Anna

AU - Willför, Stefan

AU - Rosenau, Thomas

AU - Potthast, Antje

PY - 2021/9

Y1 - 2021/9

N2 - Knowledge about the carbohydrate composition of pulp and paper samples is essential for their characterization, further processing, and understanding the properties. In this study, we compare sulfuric acid hydrolysis and acidic methanolysis, followed by GC–MS analysis of the corresponding products, by means of 42 cellulose and polysaccharide samples. Results are discussed and compared to solid-state NMR (crystallinity) and gel permeation chromatography (weight-averaged molecular mass) data. The use of the hydrolysis methods in the context of cellulose conservation science is evaluated, using e-beam treated and artificially aged cellulose samples.

AB - Knowledge about the carbohydrate composition of pulp and paper samples is essential for their characterization, further processing, and understanding the properties. In this study, we compare sulfuric acid hydrolysis and acidic methanolysis, followed by GC–MS analysis of the corresponding products, by means of 42 cellulose and polysaccharide samples. Results are discussed and compared to solid-state NMR (crystallinity) and gel permeation chromatography (weight-averaged molecular mass) data. The use of the hydrolysis methods in the context of cellulose conservation science is evaluated, using e-beam treated and artificially aged cellulose samples.

KW - Cellulose

KW - Crystallinity

KW - Electron beam irradiation

KW - Hemicellulose

KW - Methanolysis

KW - Sulfuric acid hydrolysis

KW - Historic paper

UR - http://www.scopus.com/inward/record.url?scp=85111166387&partnerID=8YFLogxK

U2 - 10.1007/s10570-021-04048-6

DO - 10.1007/s10570-021-04048-6

M3 - Article

SN - 0969-0239

VL - 28

SP - 8719

EP - 8734

JO - Cellulose

JF - Cellulose

IS - 13

ER -

Comparative hydrolysis analysis of cellulose samples and aspects of its application in conservation science

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