An approach to chemoenzymatic DKR of amines in Soxhlet apparatus

Denys Mavrynsky; Reko Leino

doi:10.1016/j.jorganchem.2013.11.005

An approach to chemoenzymatic DKR of amines in Soxhlet apparatus

Denys Mavrynsky
, Reko Leino

Tutkimustuotos: Lehtiartikkeli › Artikkeli › Tieteellinen › vertaisarvioitu

9 Sitaatiot (Scopus)

Abstrakti

The coexistence of thermolabile enzyme and metal catalyst for racemization of amines in chemoenzymatic dynamic kinetic resolution, requiring high temperature of operation, is enabled by carrying out the reaction in modified Soxhlet extraction system. Initial insights into the scope and limitations of the developed reaction system are discussed. (C) 2013 Elsevier B. V. All rights reserved.

Alkuperäiskieli	Ei tiedossa
Sivut	161–166
Sivumäärä	6
Julkaisu	Journal of Organometallic Chemistry
Vuosikerta	760
DOI - pysyväislinkit	https://doi.org/10.1016/j.jorganchem.2013.11.005
Tila	Julkaistu - 2014
OKM-julkaisutyyppi	A1 Julkaistu artikkeli, soviteltu

Keywords

Chemoenzymatic synthesis
Chiral amines
DKR
Shvo's catalyst
Soxhlet extraction

Pääsy asiakirjaan

10.1016/j.jorganchem.2013.11.005

Viittausmuodot

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title = "An approach to chemoenzymatic DKR of amines in Soxhlet apparatus",

abstract = "The coexistence of thermolabile enzyme and metal catalyst for racemization of amines in chemoenzymatic dynamic kinetic resolution, requiring high temperature of operation, is enabled by carrying out the reaction in modified Soxhlet extraction system. Initial insights into the scope and limitations of the developed reaction system are discussed. (C) 2013 Elsevier B. V. All rights reserved.",

keywords = "Chemoenzymatic synthesis, Chiral amines, DKR, Shvo's catalyst, Soxhlet extraction, Chemoenzymatic synthesis, Chiral amines, DKR, Shvo's catalyst, Soxhlet extraction, Chemoenzymatic synthesis, Chiral amines, DKR, Shvo's catalyst, Soxhlet extraction",

author = "Denys Mavrynsky and Reko Leino",

year = "2014",

doi = "10.1016/j.jorganchem.2013.11.005",

language = "Odefinierat/ok{\"a}nt",

volume = "760",

pages = "161–166",

journal = "Journal of Organometallic Chemistry",

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publisher = "Elsevier",

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TY - JOUR

T1 - An approach to chemoenzymatic DKR of amines in Soxhlet apparatus

AU - Mavrynsky, Denys

AU - Leino, Reko

PY - 2014

Y1 - 2014

N2 - The coexistence of thermolabile enzyme and metal catalyst for racemization of amines in chemoenzymatic dynamic kinetic resolution, requiring high temperature of operation, is enabled by carrying out the reaction in modified Soxhlet extraction system. Initial insights into the scope and limitations of the developed reaction system are discussed. (C) 2013 Elsevier B. V. All rights reserved.

AB - The coexistence of thermolabile enzyme and metal catalyst for racemization of amines in chemoenzymatic dynamic kinetic resolution, requiring high temperature of operation, is enabled by carrying out the reaction in modified Soxhlet extraction system. Initial insights into the scope and limitations of the developed reaction system are discussed. (C) 2013 Elsevier B. V. All rights reserved.

KW - Chemoenzymatic synthesis

KW - Chiral amines

KW - DKR

KW - Shvo's catalyst

KW - Soxhlet extraction

KW - Chemoenzymatic synthesis

KW - Chiral amines

KW - DKR

KW - Shvo's catalyst

KW - Soxhlet extraction

KW - Chemoenzymatic synthesis

KW - Chiral amines

KW - DKR

KW - Shvo's catalyst

KW - Soxhlet extraction

U2 - 10.1016/j.jorganchem.2013.11.005

DO - 10.1016/j.jorganchem.2013.11.005

M3 - Artikel

SN - 0022-328X

VL - 760

SP - 161

EP - 166

JO - Journal of Organometallic Chemistry

JF - Journal of Organometallic Chemistry

ER -