An approach to chemoenzymatic DKR of amines in Soxhlet apparatus

Denys Mavrynsky; Reko Leino

doi:10.1016/j.jorganchem.2013.11.005

An approach to chemoenzymatic DKR of amines in Soxhlet apparatus

Denys Mavrynsky, Reko Leino

Research output: Contribution to journal › Article › Scientific › peer-review

9 Citations (Scopus)

Abstract

The coexistence of thermolabile enzyme and metal catalyst for racemization of amines in chemoenzymatic dynamic kinetic resolution, requiring high temperature of operation, is enabled by carrying out the reaction in modified Soxhlet extraction system. Initial insights into the scope and limitations of the developed reaction system are discussed. (C) 2013 Elsevier B. V. All rights reserved.

Original language	Undefined/Unknown
Pages (from-to)	161–166
Number of pages	6
Journal	Journal of Organometallic Chemistry
Volume	760
DOIs	https://doi.org/10.1016/j.jorganchem.2013.11.005
Publication status	Published - 2014
MoE publication type	A1 Journal article-refereed

Keywords

Chemoenzymatic synthesis
Chiral amines
DKR
Shvo's catalyst
Soxhlet extraction

Access to Document

10.1016/j.jorganchem.2013.11.005

Cite this

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title = "An approach to chemoenzymatic DKR of amines in Soxhlet apparatus",

abstract = "The coexistence of thermolabile enzyme and metal catalyst for racemization of amines in chemoenzymatic dynamic kinetic resolution, requiring high temperature of operation, is enabled by carrying out the reaction in modified Soxhlet extraction system. Initial insights into the scope and limitations of the developed reaction system are discussed. (C) 2013 Elsevier B. V. All rights reserved.",

keywords = "Chemoenzymatic synthesis, Chiral amines, DKR, Shvo's catalyst, Soxhlet extraction, Chemoenzymatic synthesis, Chiral amines, DKR, Shvo's catalyst, Soxhlet extraction, Chemoenzymatic synthesis, Chiral amines, DKR, Shvo's catalyst, Soxhlet extraction",

author = "Denys Mavrynsky and Reko Leino",

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language = "Odefinierat/ok{\"a}nt",

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T1 - An approach to chemoenzymatic DKR of amines in Soxhlet apparatus

AU - Mavrynsky, Denys

AU - Leino, Reko

PY - 2014

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N2 - The coexistence of thermolabile enzyme and metal catalyst for racemization of amines in chemoenzymatic dynamic kinetic resolution, requiring high temperature of operation, is enabled by carrying out the reaction in modified Soxhlet extraction system. Initial insights into the scope and limitations of the developed reaction system are discussed. (C) 2013 Elsevier B. V. All rights reserved.

AB - The coexistence of thermolabile enzyme and metal catalyst for racemization of amines in chemoenzymatic dynamic kinetic resolution, requiring high temperature of operation, is enabled by carrying out the reaction in modified Soxhlet extraction system. Initial insights into the scope and limitations of the developed reaction system are discussed. (C) 2013 Elsevier B. V. All rights reserved.

KW - Chemoenzymatic synthesis

KW - Chiral amines

KW - DKR

KW - Shvo's catalyst

KW - Soxhlet extraction

KW - Chemoenzymatic synthesis

KW - Chiral amines

KW - DKR

KW - Shvo's catalyst

KW - Soxhlet extraction

KW - Chemoenzymatic synthesis

KW - Chiral amines

KW - DKR

KW - Shvo's catalyst

KW - Soxhlet extraction

U2 - 10.1016/j.jorganchem.2013.11.005

DO - 10.1016/j.jorganchem.2013.11.005

M3 - Artikel

SN - 0022-328X

VL - 760

SP - 161

EP - 166

JO - Journal of Organometallic Chemistry

JF - Journal of Organometallic Chemistry

ER -