The limit of DSC as a preliminary tool to determine the safety parameters?

A1 Originalartikel i en vetenskaplig tidskrift (referentgranskad)


Interna författare/redaktörer


Publikationens författare: Sébastien Leveneur, France Delannoy, Yoann Levesqueau, Jean-Pierre Hébert, Lionel Estel, Bechara Taouk, Tapio Salmi
Publiceringsår: 2014
Tidskrift: Chemical Engineering Transactions
Moderpublikationens namn: Book of abstracts
Seriens namn: Chemical Engineering Transactions
Volym: 36
Artikelns första sida, sidnummer: 139
Artikelns sista sida, sidnummer: 144
ISBN: 978-88-95608-27-3
ISSN: 2283-9216
eISSN: 2283-9216


Abstrakt

Safety studies are essential during the process design, but how to determine the safety parameters of a chemical process? To determine the value of safety parameters, DSC is often mentioned as a reference tool because it is safer due to the small amount of sample used. The goal of this manuscript is to illustrate the deviation between safety parameters obtained by DSC and the ones obtained by calorimetric reactor. An accident scenario, due to a cooling failure has been carried out to obtain the maximum temperature of the synthesis reaction in an open reaction system.

Senast uppdaterad 2019-22-07 vid 04:48